This general inorganic chemistry lab guide specializes in experiments involving titration and oxidation-reduction (redox) reactions. This guide aims to promote an understanding of the basic principles and practices involved in redox reactions and titration processes. Aiming to provide a holistic approach to learning, we integrate theoretical principles with practical applications. From a theoretical understanding of the principles of oxidation and reduction to the practical application of titration in chemical experiments, this guide will help you develop your skills in this area. Each lab exercise includes instructions for preparing chemical solutions, measuring and analyzing data, and questions to help you understand the theory behind each experiment. We hope this guide will be a useful tool for deepening your knowledge of inorganic chemistry and encourage you to further explore the exciting world of chemistry.